From: Subject: PowerLabs Potassium Permanganate Hypergols Date: Sat, 15 May 2004 22:10:44 +0200 MIME-Version: 1.0 Content-Type: multipart/related; boundary="----=_NextPart_000_0272_01C43AC9.777FFAD0"; type="text/html" X-MimeOLE: Produced By Microsoft MimeOLE V6.00.2800.1165 This is a multi-part message in MIME format. ------=_NextPart_000_0272_01C43AC9.777FFAD0 Content-Type: text/html; charset="Windows-1252" Content-Transfer-Encoding: quoted-printable Content-Location: http://www.powerlabs.org/chemlabs/kmno.htm PowerLabs Potassium Permanganate Hypergols

PowerLabs Potassium = Permanganate=20 Hypergols

Introduction:

Due to their spontaneous nature, hypergolic = reactions=20 can be amongst some of the most interesting to watch in chemistry. = Although there are exceptions to this, in general if two = substances are=20 reactive enough ignite spontaneously on contact chances are that = the=20 reaction will also proceed at a very high rate. Fluorine/metal = powders,=20 Alkali metals/water, Fuming Nitric Acid/Fuels, and others will all = explode=20 on contact due to the extremely high reaction rate and heat = produced=20 during the reaction. This classic high school chemistry demo shows = one=20 particularly interesting (although not very violent) hypergolic = reaction,=20 and also demonstrates that not all self initiating chemical = reactions=20 happen spontaneously:

Materials:

Reactants:	Materials:
Potassium Permanganate = (KMnO_4(s))	Hourglass
Ethylene Glycol=20 (C₂H₆O_2(l))	Eyedropper
Propylene Glycol=20 (C₃H₈O_2(l))
Glycerin (Glycerol,=20 C₃H₈O_3(l))

Procedures:

On the topic of potassium permanganate, it = should=20 also be mentioned that the reaction with hydrogen peroxide, = particularly=20 at high concentrations (50%+), is EXTREMELY violent and has been = used to=20 power turbopumps and rocket engines as the KMnO_{4 =}decomposes=20 into O₂ and Mn₃O₄, which then = goes on to=20 decompose the H₂O₂ into O₂ and=20 H₂O, with the evolution of enough heat to turn the = entire batch=20 into a blast of steam. PowerLabs hopes to develop one such engine = some=20 day, should time and machining facilities permit.
For = this demo=20 a teaspoon of potassium permanganate (a black/purple powder) = oxidizer is=20 placed in the middle of an hourglass with a small depression on it = and a=20 few drops of a liquid fuel are placed in the = depression.

Results:

Depending on the ambient temperature, the = water=20 content of the fuel, the amounts used, the degree of mixing and = the grain=20 size of the fuel the reaction may take place any time between = instantly or=20 after several minutes. With coarse grains and low ambient = temperatures=20 (this reaction is VERY temperature dependant) the reaction may = refuse to=20 take place at all until warmed up. Ethylene Glycol (caution: this = is a=20 poison) is the fastest reagent, igniting on the tested samples = within 10 -=20 20 seconds. Glycerin takes longer, at 20 - 30 seconds. Propylene = Glycol=20 took the longest, averaging over 40 seconds prior to ignition. = Once the=20 reaction starts some smoke develops and a purple flame (emission = typical=20 of excited potassium ions) erupts with the evolution of some = smoke.=20 Clicking the image will download a video showing Glycerin=20 reacting.
3.2MB, 25seconds, .mpg.

Relevant=20 Links:

Sodium=20 Peroxide Deflagration; another fine example of = hypergolic=20 reactions!
PowerLabs=20 Deflagrants overview; examples of similar reactions to = the one=20 on this page.

[ Back ] [ Home ]=20 [ Up ] [ Next ]
Comments=20 welcome: Mail me, and = tell me what=20 you think!
3D"Hit =20 People have visited this page since=20 09/04/03.
Last updated 30/01/04

Copyright =A9 1999 - 2002 by = Sam Barros. All=20 rights reserved.
Removing any material from this site for = display=20 without consent from its author consists in an infringement of=20 international copyright laws and can result in fines up to $50000 = per=20 infringement, plus legal costs. So ASK ME before you remove = anything from=20 here.

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